XRD组件

Sample Stages and Specimen Holders

Fulfilling an important role in X-ray diffraction experiments, sample stages position the specimen in the centre of the instrument, increase the degrees of freedom of diffraction space exploration and present new specimens or additional measurement spots to the beam.

布鲁克的样品阶段提供了高度的样品操纵精度。根据所需的自由度和样品尺寸的程度,可以从刺刀安装的阶段和地板安装阶段中进行选择。由于所有阶段都是Diffrac.davinci概念的一部分,因此该组件及其电动驱动器在安装时自动识别和配置。

The Universal Motion Concept (UMC) ensures that the area of interest is held in the goniometer center as the sample is moved in a myriad of directions, using up to five degrees of freedom from Phi rotation, to XYZ translation, and Psi tilt.

The bayonet mounted Eulerian cradles support applications such as stress, texture, and epitaxial thin film analysis, including at non-ambient conditions.
可以适应阶段的功能,以适应不断变化的需求。我们广泛的配件包括XY和倾斜阶段,毛细管安装座和晶圆Chucks。

Add to that Bruker’s large portfolio of specimen holders, and it’s guaranteed that any sample - whether it is inorganic or organic, available in small or large quantities, bulk or powder – can be mounted and measured with the optimal instrument configuration.

刺刀安装的阶段

The bayonet mount of the stage allows fast and accurate exchange of the entire sample stage at the goniometer for maximum experimental flexibility.

Our motorized XYZ translation stages include the Compact UMC and the Compact UMC Plus 80/150. The UMC stages are generally used for the analysis of large bulk samples, mapping applications and coating analysis, but can also be used for multiple smaller samples or to host dome temperature stages for non-ambient experiments. In addition, the Compact UMC Plus 150/80 stages have unlimited Phi rotation. The UMC 150 also includes utility feedthroughs that prevents vacuum pipe and electrical lines tangling.

刺刀固定的紧凑型摇篮(Plus)和中心的Eulerian摇篮支持应用,例如应力,纹理和外延薄膜分析,包括使用DOME温度腔室在非镜头条件下进行的。各种舞台配件甚至可以安装不规则形状的样品,并且紧凑型摇篮上的真空馈电牢固地固定在适当的位置。

紧凑型UMC

紧凑型UMCPlus 80

紧凑的摇篮

紧凑型UMCPlus 150

紧凑的摇篮Plus

Centric Eulerian Cradle

基础安装阶段

D8发现衍射仪家族可用于大型样品,以及需要繁重举重时,可在D8 Discover衍射仪家族上使用基本阶段。我们的UMC系列提供了无与伦比的映射和重量容量,可实现重达5千克的样品的大面积映射,并尺寸高达300mm。所有阶段都允许在X,Y和Z中进行机动定位和扫描样品。UMC350和UMC 1516还包括PSI-TILT,作为额外的压力,质地和外延薄膜分析的自由度。

Specialty stages are available for dedicated applications, such as the UMC 150 HTS for high throughput well plate analysis. To add even more functionality, accessories such as capillary spinners, vacuum chucks and non-ambient chambers can be mounted on top of the UMC stages. Due to their high modularity, the UMC stages can be further customized to match user requirements that go beyond standard configurations.

联电150

UMC 151

UMC 150 hts

UMC 350

UMC 150 hts-3

UMC 1516

Sample stage attachments

These components are attached on top of most materials research stages to offer simple, secure sample mounting and additional degrees of freedom. The gallery below shows a selection of available stage attachments.

Sample changers

The FLIP-STICK and AUTO-CHANGER offer a large storage capacity of up to 90 samples for completely unattended handling of batch measurements. Being fully integrated into the DAVINCI.DESIGN plug & play concept, these sample changers offer unrivalled analytical flexibility. A wide range of different specimens and specimen holders can be measured in both reflection and transmission geometry, using focusing and parallel beam optics. The magazines of the sample changers are easily exchangeable, even when loaded with samples. This allows pre-loading of additional magazines while other measurements are running, thus increasing sample throughput.

标本夹s

X射线衍射不需要任何复杂的样品准备,但取决于例如样本一致性,音量或其他属性,需要适当的标本持有人。下面显示了针对不同类型标本的众多专用解决方案的选择。

Additional Resources

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