FT-IR/Raman Training Course
概述
Description:
The FT-IR/Raman Training Course is designed for those users new to data acquisition and sample preparation. Laboratory teaching emphasizes measurement using various sampling accessories and spectral manipulations with the OPUS software. Three optional special topics are given on Thursday on specific advanced techniques.
The course will consist of lectures, laboratories sessions, and demonstrations which emphasize basic principles of FT-IR instrumentation, data processing, sampling techniques, the OPUS/IR PC software, and introductory instrument maintenance and troubleshooting.
主题：
- 概述of NIR
- Introduction to Matrix-F, process probes and accessories
- Best practices for installation and operation of inline equipment
- CMET process software
- Sampling theory
- Process (I/O) communications
- Instrument diagnostics and maintenance
- opus/cmet软件
- Basic maintenance procedures
- 与服务人员讨论betway手机客户端下载
Prerequisite:
Windows XP和Windows 7的工作知识operating system and a familiarity with your Bruker FT-IR and FT-Raman instrument. The basics aspects of the operating system (e.g. copying files, formatting disks, installing printers) can be practiced in the tutorials provided with the operating system.
Please bring your laptop with OPUS software installed if available.
Date:
June 6th- 9th, 2022
September 12th-15th, 2022
December 5th- 8th, 2022
►►► PLEASE NOTE:
这门课几乎和在t举行wo two-hour sessions each day, from 9 a.m. to 11 a.m. and from 1 p.m. to 3 p.m.
Location:
费用：
$ 1800
（包括课程材料）必威手机客户端
If your Bruker FT-IR or FT-Raman spectrometer has been installed within the last 12 months, one tuition is normally included as part of your purchase (please refer to your system quotation).
训练course syllabus
Monday:
1) Introduction to FTIR spectroscopy:
- 分子振动和光吸收
- 干涉仪：建设性和破坏性干扰
- Interferogram of monochromatic, polychromatic and broadband sources
- 一个dvantages of FTIR spectroscopy
- Principles of data processing: folding, apodization, zerofilling; phase errors
- Spectral resolution
2）FTIR光谱仪的光学组件：
- Sources
- Beamsplitters
- Detectors
- Windows
- Mirrors
- Polarizers
- Optical filters
3) FTIR Sampling Techniques:
- Transmission
- Reflectance
- DRIFT
- 一个TR
4）光谱解释：
- 一个lkanes, phenols, ethers, ketones, acids, etc.
5) FTIR test protocols:
- Validation test setup
- Running OVP tests
6) Instrument care:
- Basic maintenance and troubleshooting
- Optical components exchange
Tuesday:
1）拉曼简介：
- Infrared vs. Raman spectroscopy
- Dependency of the excitation line
- 尖峰校正
- Fluorescence and thermal background
2）Opus I：基本功能和数据采集：
- Software overview
- 文件结构
- 使用文件
- Setting experimental parameters
3) Lab session I, data acquisition:
- 光谱分辨率的影响
- Effect of apodization function
- Effect of zerofilling
- Effect of number of scans and S/N evaluation
4）Opus II：数据操纵和评估：
- Base line correction
- Spectral subtraction
- 库搜索
- Plotting spectra
- Quantitative analysis
5）实验室会议II，数据操作：
- 导出数据
- Peak picking
- Plotting with peaks
- Baseline correction
- Spectral subtraction
- Plot layout editor
周三：
1) Lab session II continued
2) OPUS 3D:
- 3D file structure
- Chemical image
- Extract spectra
3) OPUS 3D lab session
4）定量分析：
- 作品量I和II
- Selecting of samples
- PLS data modelling
Optional sessions (Thursday)
1）快速扫描和阶梯扫描时间分辨光谱学：
- Principles of rapid- and step scan FTIR
- 组件：探测器，数字化器，过滤器
- Parameters optimization
- 触发
- Examples
- 实验室演示
2) Microscopy:
- 概述
- Sample visualization
- Sample preparation
- 传输，反射率，ATR和放牧角技术
- 解析度
- Mapping and imaging
- 实验室会话
3) Raman spectroscopy:
- Principles of Raman spectroscopy
- Side effects: fluorescence and thermal emission
- Selection of excitation laser
- ft与色散拉曼光谱
- 拉曼显微镜
- 实验室会话