Elexsys.

ELEXSYS-II E600/680

94 GHz的高频/高场EPR和ENDOR

The ELEXSYS family of EPR spectrometers now includes two W-band systems, the E600 and E680. The former is optimized for CW-EPR experiments at 94 GHz, while the E680 operates in both CW- and FT-mode. These high-class research instruments provide a maximum in performance and flexibility while still being easy to operate. Thus all of the advantages of high frequency EPR become readily accessible.

This setup provides an accurate final operating frequency - a must for all g-factor measurements. Flexibility in the system is assured by the modular architecture, allowing the system to be setup as a CW or a combined FT/CW instrument. System operation can be switched from CW to FT or even from W-Band to X-Band at the push of a button. The variable-temperature W-band TeraFlex probehead operates from 4 K to 300 K.

样品可以在任何温度下交换。高精度腔匹配,调谐和样品定位力学促进高样品吞吐量,易于处理。对于桥接和谐振器调整400 MHz宽调谐显示并在IF上检测到。所有这些硬件功能都是由XEPR软件的补充,其中易于学习的图形用户界面。

主要特点

W-Band bridge
  • Precise microwave power setting over a 60 dB range in W-band
  • All FT-EPR relevant parameters such as pulse power, width and phase are set and monitored on the intermediate frequency (IF) at X-band
  • High spectral purity and sensitivity are achieved by the combination of a fixed frequency oscillator and a PLL circuit

Additional Features

  • The high magent field required for W-band operation requires a superconducting magnet, however not all superconducting magnets are sutiable for EPR. Thus the EPR 6T SC was developed with EPR spectroscopy in mind.
  • As high frequency EPR, in particular pulse EPR, has evolved so have the desires of the EPR spectroscopist. Depending on the pulse EPR experiment, certain advantages are available with more microwave power. For such situations, we offer two W-band bridge upgrades.

技术细节

•94 GHz operation frequency

•CW and FT operation

•ELDOR and ENDOR

•100 MW,400 MW和2 W电源选项

•单模谐振器

•Sample temperature: 4-300 K

•Superconducting magnet

  • 6 T main coil
  • 0.2 T扫线圈

Testimonials

Advantages of High Frequency EPR

MW-Nutation of Coal Sample at 94 GHz. The nutation period is 62 ns with the 400 mW High Power Upgrade unit.
  • Increase in spectral resolution due to the higher magnetic field.
  • 由于较高的谐振器填充因子,有限量的样品的检测灵敏度的增加。
  • 增加在investi方向选择性gation of disordered systems.
  • Accessibility of spin systems with larger zero-field splitting due to the larger microwave quantum energy.
  • Better separation of the ENDOR spectra of different nuclei.
  • Improvement in the ENDOR detectability of low-frequency nuclear spins.
  • Simplification of spectra due to the reduction of second-order effects at high fields.

EPR 6T SC: The W-Band Superconducting Magnet

EPR 6T SC: The W-Band Superconducting Magnet

The second generation of W-band superconducting magnet features a horizontal field, a main coil with 6 T sweep range, permanent leads and a 2 kG high resolution sweep coil. The state-of-the-art magnet design features permanent leads for the main coil and sweep coil with a longer helium hold time compared to similar designs. Both, main and sweep-coil are connected to the newly developed power supply. Easy and safe operation is accomplished by a new software interface which allows switching between the two operation modes just by a mouse click.

W波段桥大功率升级

4-Pulse DEER time traces: 400 mW High Power Upgrade (red, upper) and 100 mW High Power Upgrade (green, lower)

对于脉冲EPR测量,其中需要短脉冲和大励磁带宽(ESEEM,鹿和FT),提供了三个W波段桥梁升级:2 W,400 MW和100 MW高功率升级。具有标准W波段谐振器的400 MW高功率升级实现脉冲长度(90o) of 16 ns. While the 100 mW High Power Upgrade routinely achieves pulse lengths (90o)40 ns。
The benefits of the 400 mW High Power Upgrade are easily observed in the 4-pulse DEER Experiment. The shorter pulse lengths lead to a higher signal to noise in the DEER spectrum which translates to a decrease in measuring time when compared to the longer pulses needed with the 100 mW High Power Upgrade.

Labscape

Service & Life Cycle Support for Magnetic Resonance and Preclinical Imaging

布鲁克’s commitment to provide customers with unparalleled help throughout the buying cycle, from initial inquiry to evaluation, installation, and the lifetime of the instrument is now characterized by the LabScape service concept.

LabScape Maintenance Agreements, On-Site On-Demand and Enhance Your Lab are designed to offer a new approach to maintenance and service for the modern laboratory

More Informations