3D X-ray Microscopy (XRM)

Skyscan 2214

3D X-ray Microscopy at the Nanoscale

Ultimate Performance at your Command

herostageskyscan2214

Punti Salienti

权力,分辨率,视野

300 x 400 mm
largest size that can be accommodated
Whether the sample is enormous or small, the SKYSCAN 2214 has the flexibility to image them all.
160 keV
penetrating power
曲ick change filament for switching between W for highest penetration or LaB₆ for highest resolution
<500 nm
真3D空间分辨率
There are many ways to define resolution, but the most important is the ability to resolve 2 features in the resulting 3D model.

Watch the video to get more insight

Skyscan 2214 - 纳米级X射线显微镜

The new MULTISCALE X-ray nanotomograph SKYSCAN 2214 covers the widest range of object sizes and spatial resolutions in a single instrument. It opens unique possibilities for 3D imaging and exact modeling of geological materials in oil and gas exploration, composite materials, Li batteries, fuel cells, electronic assemblies, as well as ex-vivo preclinical applications like in lung imaging or tumour vascularization.

The instrument allows scanning and 3D non-destructive reconstruction of the internal microstructure of objects as large as >300mm in diameter as well as submicron resolution for small samples.

The system contains an "open type" transmission X-ray source with <0.5 microns spot size and a diamond window. It can be equipped with up to four X-ray detectors for maximum flexibility: flat-panel for large objects, 11Mp cooled CCD with wide field of view, 11Mp cooled CCD with medium field of view, 8Mp cooled CCD for highest spatial resolution. Automatic variable acquisition geometry and phase-contrast enhancement allows best possible quality in relatively short scanning time.

Skyscan 2214is complemented by 3D.SUITE. This comprehensive software suite covers GPU-accelerated reconstruction, 2D/ 3D morphological analysis, as well as surface and volume rendering visualization.

Caratteristiche

Key Features

Skyscan 2214Features

Source

2214使用最新一代open-typ SKYSCANe X-ray source. The source offers true spatial resolution below 500 nm, an X-ray energy up to 160 keV and source power up to 16 W. The source is practically maintenance-free with an extremely easy pre-aligned filament replacement procedure.

Skyscan 2214具有带有钻石窗口的开放型(泵送)纳米焦X射线源。它产生的X射线束从20 kV到160 keV,并提供两种类型的阴极。钨(W)阴极在最高160 kV的整个加速电压下运行,并提供一个斑点尺寸降至800 nm。甲状腺六角杆(LAB6)阴极可用于将电压从20 kV加速至100 kV,并提供小于500 nm的X射线束的斑点,以实现成像和3D重建方面的最高分辨率。JIMA分辨率模式表明500 nm结构可以轻松解析。

为了使焦点斑点大小和发射点位置的长期稳定性,X射线源配备了液体冷却系统,该系统包含重新循环器,可提供冷却液的精确温度稳定性。

Skyscan 2214Features

探测器

The SKYSCAN 2214 can be equipped with up to four X-ray cameras for ultimate flexibility: three CCD cameras with different resolution and field of view and one large-area flat panel detector. All cameras can be selected with a single mouse click. The different CCD cameras can be retro-fitted at any point of time during the system’s lifetime.

所有三个CCD都可以在中央梁位置和两个偏移位置拍摄图像,以使视场的视野增加一倍。两个偏移位置中的图像将自动缝合,并补偿偏移和可能的强度差异。

Using CCD detectors with small pixel size allows extension of high-resolution imaging and 3D reconstruction to large objects. The built-in detector flexibility enables adjusting the field of view and spatial resolution according to the object size and density. An advanced reconstruction from a volume of interest provides scanning of a selected part of a large object with high resolution without compromising image quality.

Additionally, the field of view can be increased horizontally and vertically by using offset camera positions and vertical object movement.

Skyscan 2214Features

In-situ stages

The high-precision object stage of the SKYSCAN 2214 supports objects up to 300 mm diameter and 20 kg in weight. The air-bearing rotation motor allows precise rotation of objects at very high accuracy, and the integrated micro-positioning stage guarantees a perfect sample alignment.
The SKYSCAN 2214 has a large and easily accessible sample chamber to allow scanning of big objects as well as mounting of optional stages. On top plenty of space is available for peripheral equipment.

The Bruker material testing stages are designed to perform compression experiments up to 4400 N and tensile experiments up to 440 N. All stages automatically communicate through the system’s rotation stage, without the need of any cable connections. Using the supplied software, scheduled scanning experiments can be set up.

布鲁克's heating & cooling stages can reach temperatures of up to +80 °C or 30 °C below ambient temperature. Just like the other stages, no extra connections are needed, and there is an automatic recognition of the stage. Using the heating & cooling stages, samples can be examined under non-ambient conditions, to evaluate the effect of temperature on the sample’s microstructure.

The SKYSCAN 2214 is fully compatible with stages from DEBEN. With the included adapter, the DEBEN stage can be simply placed onto the rotation stage of the SKYSCAN 2214.

Cooling Stage
Material Testing Stage
Deben Stage

Applicazioni

Highlighted Applications

Skyscan 2214Applications

添加剂制造

添加剂制造, also commonly called 3D printing, allows the creation of components with complex external and internal structure. Unlike classic techniques which require special molding or tooling, additive manufacturing allows the economical production of both one piece prototypes and large batch production parts. Once completed, confirmation of both the internal and exterior structure is important in ensuring that the component will perform as intended. XRM allows this inspection in a non-destructive manner, giving confidence that a component will meet or exceed specifications.

  • 检查被困粉的内部空隙
  • Validation of external and internal dimensions
  • Direct comparison with CAD models
  • 单一和多物质组件的分析
Skyscan 2214Applications

Fibers and composites

通过将材料组合到复合材料中必威手机客户端,所得组件的强度可以增加,同时显着减少了重量。进一步的优化来自确保优化子组件的方向。使用的经典组件之一是纤维,从混凝土中的钢钢筋到航空材料中的碳纳米管。必威手机客户端XRM允许检查纤维和复合材料,而无需横截面,确保样品的状况不受样品准备的影响。

  • 嵌入对象的方向
  • 曲antification of layer thickness and fiber sizes
  • In-situ temperature and physical properties testing with accessory stages
Skyscan 2214Applications

地质学

The study of geological specimens, whether it is a core sample from deep below the surface or a rock laying on the ground, offers a wealth of information into the formation of the world around us. Analysis often requires destruction of the pristine sample, removing important provenance of the internal structures. XRM gives a view into the sample without sectioning, allowing faster time to result and the possibility of future analysis.

  • Density dependent 3D visualization of the specimen interior
  • Pore network visualization
  • Digital sectioning allowing application standard geological methods

Specifiche

Skyscan 2214规格

Feature

规格

Benefit

X-ray source

20-160 kV

16 W max.

User exchangeable filament

Optimize for max power (W) or max resolution (LaB6)

Rotatable diamond window for maximum lifetime

X-ray detector

6 MP活动像素平板板

11 Mp large format cooled CCD

11 Mp mid format cooled CCD

8 MP HI-RES冷却CCD

Variety of pixel and detector sizes allow balance between detector resolution, coverage and counting statistics

可提供1、2、3或4个检测器

Field upgradable to add detectors

图像格式

Up to 8000 x 8000 x 2300 pixels after a single scan

User selectable image size allows balance of dataset size and needed resolution

数据收集后软件允许裁员

Resolution

60 nm smallest pixel size
<500 nmlow-contrast resolution (10% MTF)

Simple graphics control for optimizing experiment resolution based on selected detector, sample and detector distance

Adjustable source focus size to balance maximum power and resolution

定位准确性

<50 nm for rotation
Anti-vibration granite platform with pneumatic leveling

空气轴承样品阶段提供平稳的旋转

Simple chuck style mounting of sample posts

高级材料研究阶段的机械和电界面必威手机客户端

Maximum Object Size

直径为300毫米(140毫米扫描尺寸)

400 mm in length

最大物体重量20公斤

Both the power and room to scan large samples

Precise positioning of small samples near the source to maximize magnification

Dimensions W 1800毫米X D 950毫米X H 1680毫米

重量:1500公斤

Efficiently designed to optimize use of lab space

Source maintenance access via interlocked large sliding door

Software

POSITION, SCAN, RECONSTRUCT and ANALYZE

XRM Software

布鲁克XRM solutions include all software needed to collect and analyze data. An intuitive graphical user interface with user guided parameter optimization support both expert and novice users. By using the latest GPU powered algorithms, reconstruction time is substantially reduced. CTVOX, CTAN and CTVOL combine to forma powerful suite of software for both qualitative and quantitative analysis of models.

Measurement Software:
Skyscan 2214 - 仪器控制,测量计划和收集

Reconstruction Software:
NRECON – Transforms the 2D projection images into 3D volumes

Analysis Software:
DATAVIEWER– Slice-by-slice inspection of 3D volumes and 2D/3D image registration
CTVOX– Realistic visualization by volume rendering
CTAN– 2D/3D image analysis & processing
CTVOL- 可视化表面模型以导出CAD或3D打印

网络研讨会

Supporto

Service & Support

我们提供:

  • Help desk support from highly-skilled troubleshooting professionals, to isolate and resolve hard- and software problems
  • Web-based remote instrument service for service diagnosis and applications support
  • 合并现实支持 - 您身边的虚拟工程师(视频)
  • Planned maintenance, according to your requirement
  • 客户现场维修和保养服务betway手机客户端下载
  • 备件的可用性通常在全球的几个工作日或几个工作日之内
  • Compliance services for installation qualification, operational qualification / performance verification
  • 现场计划和搬迁
  • 找到您的下一个训练课程

Check out oursupport websitefor:

  • 软件更新
  • Product manuals & installation guides
  • 培训视频

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