CS/ONH-Analysis (CS/ONH)

G8 GALILEO

High-end analyzer, designed for automatic and precise determination of O/N/H

The most versatile system available

质谱检测能力

HerostageG8GALILEO

Основные моменты

High-end designed for accuracy @ high-throughput

ppb(ng/g)
Limit of Detection
G8 Galileo中使用的所有最先进的检测器均配备内部参考通道,以实现最大稳定性,并允许在子PPM范围内进行检测极限(基于1G样品质量)
3+ analyzers
In one single system
Whether the task is O/N/H analysis with real H2-detection by TCD, reliable sub-ppm determination of H in high purity Al, diffusible & residual Hydrogen in welds, or argon inclusion analysis of powder feedstock for additive manufacturing, or in final parts: the G8 GALILEO can be equipped to fulfill almost every analytical challange.
0-100 amu
m/z range of mass spectrometer (MS)
The industrial-grade MS is tailor made for hydrogen and argon detection, equipped with an optimized ion source and channeltron detector. With an extremely efficient gas inlet system, it delivers detection limits in the lower ng/g range, equivalent to a particle density of a few molecules.

Matching the best ONH method - Inert Gas Fusion - with the ideal ONH systems: G8 GALILEO and G8 GALILEO MS

温度重要:普通金属及其氧化物,硝酸盐和氢化物的熔点

With the G8 GALILEO analyzers, Bruker is the only company to offer fully integrated ONH solutions combining the benefits of multiple dedicated systems without any analytical compromise or technical limitations. The G8 GALILEO applies the Smart Molecule Sequence™ for direct measurement of all emitted gases and real 1:1 information - without chemical transformations, mathematical corrections or unpublished algorithms. FusionControl, the ongoing contact free temperature measurement of the sample ensures the right analysis temperature, avoiding formation of interfering products and increasing stability and uptime.

Options for automatic sample and crucible handling, electrode cleaning and automatic gas dose calibration are available. When equipped with the unique IR-furnace of theG4凤凰,执行可靠的扩散,残留和总氢测量,并符合ISO 360和AWS A4.3焊接标准。

关键好处:

  • Advanced water cooled electrode furnace with FusionControl, water cooled sample port, high capacity dust trap, followed by efficient in-line particle filtering
  • Smart Molecule Sequence: Direct and unadulterated measurements of all emitted gases by state-of-the-art detectors with reference channels
  • Automatic furnace cleaning, crucible and sample handling available
  • 可用的可扩散氢确定的独特外部IR费用
  • Automatic and reliable gas calibration with 10 different volumes available
  • Thermal Desorption Mass Spectroscopy (TDMS) and argon inclusion analysis available by MS coupling

Особенности

преим联щL

Why do I need Inert Gas Fusion Analysis?

The three non-metals Oxygen (O), Nitrogen (N) and Hydrogen (H) determine the quality, service life and mechanical properties of all metallic materials. Unlike metallic alloy components, the amount of O, N and H sometimes changes considerably along the entire process chain, from the production of raw materials to the completion of the finished product. Similar applies to argon inclusions, introduced at trace level during metal powder production by atomization that will remain in the final product.
Acquiring kinetic information about diffusible hydrogen and its damaging mechanisms are further examples with actual backgrounds like development of new generations of high strengths steels, materials suitable for hydrogen storage or biomedical implants.

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Powder Metallurgy and Additive Manufacturing

在添加剂制造和其他粉末冶金过程中使用的金属粉末是具有严格定义颗粒特性的高纯度材料。必威手机客户端它们的较大特异性表面使它们容易受到沿生产链的氧化/水分“衰老”,其氧气和氢含量主导了产量率和产品质量。现成的G6 Leonardo解决了此类新兴工业应用的需求。必威东盟体育

Glass & Ceramics

From industry refractory materials to high performance ceramics in electronics or in metal cutting, refractory oxides, nitrides and carbides have a wide usage. The unique properties of glass and ceramics are influenced in fundamental ways by the level of oxygen, nitrogen and hydrogen present in the process or in the final product. With SampleCare™, FusionControl and its robustness, the G6 LEONARDO is an excellent tool for the fast analysis of raw materials, intermediates and final products.

Welding and allied Processes

Bruker’s unique G8 GALILEO IR is supported by ISO 3690 and AWS A4.3 and enables a rapid assessment of diffusible hydrogen levels introduced during welding. Because of its speed, it enables pre-welding experiments on test samples, helping the welding industry to avoid costly failures.

Thermal Desorption Mass Spectrometry

带有温度坡道的热解吸质谱(TDM)提供了动力学信息,例如金属结构中氢的捕获能量。诸如可扩散,弱或强的术语之类的术语,化学结合的氢可以与所提供的活化能直接相关。布鲁克(Bruker)独特的G8伽利略MS能够以几种ng/g的浓度分析氢或同位素等同位素。这使得开发适合氢储存的新合金世代或合金所需的精确机制研究。

Спецификации

G8 GALILEO Specifications

Specification 益处

Detectors

Oxygen
CO的非分散性红外吸收,无运动部件,带有参考光束的双范围检测器和板上线性化 Reliable, maintenance-free performance without drift
氮和氢 Thermal conductivity detector with reference channel and adjustable gain amplifier Reliable, adjustable ranges, drift free
Argon and Hydrogen 质谱仪1-100 AMU,单四极杆,优化的EI源和Channeltron检测器 Unique mass spectrometry performance, sensitivity: a few molecules
载气 He(O,n),AR(O,N),N2(H)纯度为99.995%(痕量分析99.9990%) 无妥协的柔性载气选择
校准气体 Pure gases or certified mixtures (99.999 % for each compound), 10 individual volumes in the gas dose device to cover a huge range Easy, precise gas calibration without standards, directly tracable to fundamental
parameters (pressure, temperature, volume)
Sample Dimensions 电极炉:8 x 8毫米横截面(碎片,芯片,销钉,颗粒),可用于特殊应用的样品端口
冷却水 电极炉:4 l / min3 bar supply pressure IR Furnace: 1 l/min at 3 bar supply pressure, 15 – 20 °C inlet temperature, 100 – 240 V / 50 – 60 Hz 适合每条通常的自来水管线,带电磁阀的自来水储蓄设计,冷却器也可能

电源

G8 GALILEO
400 - 480 VAC(±10%),50 - 60 Hz,32 a,7 kVa,1相加N或2相,接地线
质谱仪(MS) 230 VAC, 50 – 60 Hz, 250 VA Flexible, worldwide power and current configurations
External Infrared Furnace 230 VAC,50 - 60 Hz,1,500 VA Flexible, worldwide power and current configurations
尺寸及重量
G8 GALILEO 80 x 60 x 83厘米(w x d x H),〜130 kg*)
Mass Spectrometer
63 x 64 x 48 cm (W x D x H), ~60 kg
External Infrared Furnace 48 x 66 x 30厘米(w x d x h),〜15 kg
*) Depending on configuration

Вебинары

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